WARNING NOTICE
The experiments described in these materials are potentially hazardous and require a high level of safety training, special facilities and equipment, and supervision by appropriate individuals. You bear the sole responsibility, liability, and risk for the implementation of such safety procedures and measures. MIT shall have no responsibility, liability, or risk for the content or implementation of any of the material presented.
Legal Notice
The experiments for 5.311 have evolved over a period of many years and include contributions from past instructors, course textbooks, and others affiliated with the course. For many of these lab documents, no single source can be attributed. Dr. Mircea Gheorghiu is the primary author of certain documents, as noted below. Additionally, he designed the experiment for ionic liquid acylation of ferrocene. In the Unknown Aromatic Carboxylic Acid experiment, Dr. Gheorghiu authored the section on calculating the second derivative and Gran's plot.
Labs files.| EXPERIMENTS | APPENDICES |
|---|
| Kinetics (PDF) (Courtesy of Dr. Mircea Gheorghiu. Used with permission.) | |
| NMR (PDF) | Appendix (PDF) (Courtesy of Dr. Mircea Gheorghiu. Used with permission.) |
| Unknown Aromatic Carboxylic Acid (PDF - 1.0 MB) | Appendix 1 (PDF) (Courtesy of Dr. Mircea Gheorghiu. Used with permission.)
Appendix 2 (PDF) |
| Preparation of Ferrocene and Acetylferrocenes (PDF - 1.5 MB) | Appendix 1 (PDF) (Courtesy of Dr. Mircea Gheorghiu. Used with permission.)
Appendix 2 (PDF) (Courtesy of Dr. Mircea Gheorghiu. Used with permission.) |